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Product Details
Factory supply 2-Nitroresorcinol 601-89-8 with low price
- Molecular Formula: C6H5NO4
- Molecular Weight: 155.11
- Appearance/Colour: orange crystalline powder
- Vapor Pressure: 0.0184mmHg at 25°C
- Melting Point: 81-83 °C(lit.)
- Refractive Index: 1.5423 (estimate)
- Boiling Point: 245.3 °C at 760 mmHg
- PKA: 4.88±0.10(Predicted)
- Flash Point: 111.4 °C
- PSA： 86.28000
- Density: 1.58 g/cm3
- LogP: 1.52920
2-Nitroresorcinol(Cas 601-89-8) Usage
|
Purification Methods |
Recrystallise 2-nitroresorcinol from aqueous EtOH. [Beilstein 6 H 823.] |
InChI:InChI=1/C6H5NO4/c8-4-2-1-3-5(9)6(4)7(10)11/h1-3,8-9H/p-2
601-89-8 Relevant articles
Sodium perborate/NaNO2/KHSO4-triggered synthesis and kinetics of nitration of aromatic compounds
Rajanna,Muppidi, Suresh,Pasnoori, Srinivas,Saiprakash
, p. 6023 - 6038 (2018/09/21)
Sodium perborate (SPB) was used as effic...
A phenol compound green nitration method and application
-
Paragraph 0052; 0053; 0054; 0055; 0556; 0057; 0058; 0059, (2017/08/24)
The invention discloses a green nitrific...
Environment-friendly bionic catalytic nitration method for phenolic compound
-
Paragraph 0045-0046, (2017/06/19)
The invention discloses an environment-f...
Biomimetic Nitration of Phenols Using Metalloporphyrins/H2O2/NO2 -
Sun, Weizhi,Liu, Yaojie,Zhang, Haibo,Xian, Mo,Liu, Huizhou
, p. 1991 - 1999 (2015/12/24)
An efficient metalloporphyrins/H2O2/NO2 ...
601-89-8 Process route
-
-
108-46-3
recorcinol
-
-
601-89-8
2-nitroresorcinol
| Conditions | Yield |
|---|---|
|
With
antimony trinitrate;
In
water;
for 0.0166667h;
Cooling;
|
95%
|
|
With
potassium hydrogensulfate; sodium perborate hexahydrate; sodium nitrite;
In
neat (no solvent);
for 0.0208333h;
regioselective reaction;
Molecular sieve;
Microwave irradiation;
|
75%
|
|
recorcinol;
With
sulfuric acid;
at 20 ℃;
Heating;
With
sulfuric acid; nitric acid;
In
water;
Cooling with ice;
Reflux;
|
60%
|
|
With
sulfuric acid; sulfur trioxide;
anschliessend Behandeln mit HNO3;
|
|
|
With
sulfuric acid;
at 60 - 100 ℃;
Behandeln mit einem Gemisch von konz. Schwefelsaeure und Salpetersaeure bei 60-70grad und anschliessendes Einleiten von Wasserdampf;
|
|
|
With
sulfuric acid; acetic acid;
Behandeln des Reaktionsprodukts mit Salpetersaeure in Eisessig bei 0grad und anschliessendes Einleiten von ueberhitztem Wasserdampf;
|
|
|
With
sulfuric acid;
Nitrieren des Reaktionsprodukts mit HNO3 und rauchender Schwefelsaeure und mit Schwefelsaeure erhitzen;
|
|
|
With
sulfuric acid;
at 60 - 100 ℃;
Behandeln mit einem Gemisch von konz. Schwefelsaeure und Salpetersaeure bei 25grad und anschliessendes Einleiten von Wasserdampf;
|
|
|
With
potassium hydrogensulfate; thorium(IV) nitrate pentahydrate;
In
acetonitrile;
at 82 ℃;
for 0.416667h;
regiospecific reaction;
|
87 %Chromat.
|
|
With
thorium(IV) nitrate pentahydrate;
In
acetonitrile;
at 82 ℃;
for 0.416667h;
regiospecific reaction;
|
87 %Chromat.
|
-
-
108-46-3
recorcinol
-
-
3163-07-3
4-nitroresorcinol
-
-
601-89-8
2-nitroresorcinol
| Conditions | Yield |
|---|---|
|
With
dihydrogen peroxide; sodium nitrite;
In
aq. phosphate buffer;
at 20 ℃;
for 1.58h;
pH=7;
Reagent/catalyst;
Concentration;
Green chemistry;
|
27.4%
23.5% |
|
With
5,10,15,20-tetraphenyl iron porphyrin; C44H28FeN4O12S4; dihydrogen peroxide; sodium nitrite;
at 20 ℃;
for 1.33333h;
pH=7;
Reagent/catalyst;
|
10.9%
13% |
|
With
tetrasodium 5,10,15,20-tetra(4-sulfophenyl)porphyrinatoiron(II); dihydrogen peroxide; sodium nitrite;
In
aq. phosphate buffer;
at 25 ℃;
for 1.33333h;
pH=7;
regioselective reaction;
Green chemistry;
|
11.8 %Chromat.
9.9 %Chromat. |
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