Product Details
Manufacturer supply top purity CIS-3-CHLOROACRYLIC ACID 1609-93-4 with GMP standards
- Molecular Formula: C3H3ClO2
- Molecular Weight: 106.509
- Appearance/Colour: White crystals
- Vapor Pressure: 0.216mmHg at 25°C
- Melting Point: 61-62 °C(lit.)
- Refractive Index: 1.4100 (estimate)
- Boiling Point: 192.3 °C at 760 mmHg
- PKA: pK1: 3.32 (18°C,μ=0.1)
- Flash Point: 70.1 °C
- PSA： 37.30000
- Density: 1.371 g/cm3
- LogP: 0.82350
CIS-3-CHLOROACRYLIC ACID(Cas 1609-93-4) Usage
InChI:InChI=1/C3H3ClO2/c4-2-1-3(5)6/h1-2H,(H,5,6)/p-1/b2-1-
1609-93-4 Relevant articles
One-pot Synthesis of α,β-Butenolides from Methyl (Z)-3-Chloroacrylate
Barluenga, Jose,Fernandez, Jose R.,Yus, Miguel
, p. 183 - 184 (1986)
A one-pot synthesis of 4,4-disubstituted...
Hydrochlorination of 2,3-acetylenic acids with thionyl chloride in dimethylformamide
Urdaneta, Neudo A.,Herrera, Julio C.,Salazar, Jose,Lopez, Simon E.
, p. 3003 - 3009 (2002)
The reaction of 2,3-acetylenic acids (1a...
FUSED PYRIMIDINE COMPOUNDS, COMPOSITIONS AND MEDICINAL APPLICATIONS THEREOF
-
Paragraph 0282, (2021/04/02)
The present disclosure relates to a clas...
QUINAZOLINE DERIVATIVE, PREPARATION METHOD THEREFOR, AND PHARMACEUTICAL COMPOSITION AND APPLICATION THEREOF
-
Paragraph 0278; 0279, (2017/07/14)
Disclosed are a quinazoline derivative, ...
A general access to optically pure epoxypolyynes: Asymmetric synthesis of antifeedant natural products
Grandjean,Pale,Chuche
, p. 5225 - 5236 (2007/10/02)
A general asymmetric approach toward cis...
1609-93-4 Process route
-
-
471-25-0
Propiolic acid
-
-
1609-93-4
3-chloroacrylic acid
| Conditions | Yield |
|---|---|
|
With
acetic acid; lithium chloride;
at 70 ℃;
for 24h;
|
89%
|
|
With
acetic acid; lithium chloride;
at 70 ℃;
|
89%
|
|
With
hydrogenchloride;
copper(l) chloride;
at 0 ℃;
for 10h;
|
78%
|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 25 ℃;
for 1h;
Inert atmosphere;
|
62.9%
|
|
With
hydrogenchloride; water;
|
|
|
With
hydrogenchloride; copper(l) chloride;
|
|
|
With
hydrogenchloride; copper(l) chloride;
|
-
-
471-25-0
Propiolic acid
-
-
2345-61-1
(E)-3-chloroacrylic acid
-
-
1609-93-4
3-chloroacrylic acid
| Conditions | Yield |
|---|---|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 30 ℃;
for 0.75h;
|
31%
40% |
|
With
hydrogenchloride;
at 60 ℃;
|
|
|
With
thionyl chloride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.75h;
|
1609-93-4 Upstream products
-
471-25-0
Propiolic acid
-
107-19-7
propargyl alcohol
-
7647-01-0
hydrogenchloride
-
98021-69-3
acetic acid-(1-bromo-3,3-dichloro-propyl ester)
1609-93-4 Downstream products
-
114380-07-3
3c -(4-nitro-phenylselanyl)-acrylic acid
-
2345-61-1
(E)-3-chloroacrylic acid
-
15905-30-3
β-(phenylseleno)acrylic acid
-
706-01-4
(2Z)-3-(phenylthio)acrylic acid
CIS-3-CHLOROACRYLIC ACID
CAS:1609-93-4
Purity:99%
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